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After 5 min, the peptides were eluted and separated on the analytical column (nanoEase MZ HSS T3 Column, 100 Å, 1.8 µm, 75 µm × 250 mm, Waters) for 105 min at 250 nl/min flow rate in a 3 to 40% non-linear acetonitrile gradient in 0.1% formic acid
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